The solution 1 H NMR spectrum of the tetrahedral cluster exhibits the following signals at room temperature:

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The solution 1H NMR spectrum of the tetrahedral cluster

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exhibits the following signals at room temperature: δ/ppm 0.53 (s, 36H), 1.41 (m, 8H), 2.25 (s, 24H), 2.36 (s, 24H), 3.59 (m, 8H), 4.29 (quintet, J89Y1H 15.3 Hz, 8H). Assign the signals in the spectrum, and rationalize the appearance of the signal at δ 4.29ppm. [Data: 89Y, 100% abundant, I = 1/2.]

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Inorganic Chemistry

ISBN: 9781292134147

5th Edition

Authors: Catherine Housecroft

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