ssEach of the following reactions has been reported in the chemical literature and proceeds in good yield.
Question:
(a)
(b)
(c)
(d)
(e) Product of part (d) + HCl †’
(f)
(g)
(h)
(i)
(j)
(k)
(l)
(m)
(n)
(o)
(p)
(q)
(r)
(s)
Transcribed Image Text:
H. Pt 1,2-Diethyl-4-nitrobenzene to 1,3-Dimethyl-2-nitrobenzene . SnCl, HCL -, 2.. Ho Pales dpereo 0 Product of part (b) + CICH2CCI Product of part (c) (CH,CH3)2NH CoHsNHCCHCH.CH HO 1, LiAIHA 2, но Aniline +heptanal N AICI Acetanilide CICH2CCI AIC Acetanilide CICH2CCI NaNO,, H SO, HO Product of part (i) 2. H-0, heat 2,6-Dinitroaniline 2. CuCI l NaNO, HBr, H-O 2 CuB o-Nitroaniline NaNO HCI H.O . HCL H- 2. CuON 2,6-Diiodo-4-nitroaniline I. NaNO,, HSO. HO 2. KI heut 2.4.6-Trinitroaniline PO. NaNO2, HSO H-0, H,PO 2-Amino-5-iodobenzoic acid 2 CHCH,OH I. NaNO. HSO. H2O Aniline 2 23,6-trimethylphenol I. NaNO, HCL. HO 2. HO (CH)2N CHs
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a Catalytic hydrogenation reduces nitro groups to amino groups b Nitro groups are readily reduced by tinII chloride This reaction is the first step in a synthesis of the drug lidocaine c The amino gro...View the full answer
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