Question: 1. Using the NMR spectra, create a prediction table showing shift, integrations, and splitting 2. Compare NMR spectra with what was expected. Are there any

1. Using the NMR spectra, create a prediction table showing shift, integrations, and splitting

1. Using the NMR spectra, create a prediction table showing shift, integrations,

2. Compare NMR spectra with what was expected. Are there any contaminants?

and splitting 2. Compare NMR spectra with what was expected. Are there

NMR expected spectra

zoom into the picture

-7.21 1.98 -1.88 -1.79 -10000 -9000 -8000 7000 -6000 -5000 -4000 3000 +2000 +1000 -0 T T 5-761 7.2 7.0 6.8 .6 6.4 6.2 6.0 5.8 5.6 5.4 5.2 5.0 4.8 4.6 4.4 4.2 4.0 3.8 3.6 3.4 3.2 3.0 2.8 2.6 2.4 2.2 2.0 1.8 1.6 f1 (ppm) +-1000 1.4 1.2 1.0 Proton NMR for the product in the Intro to Substitution experiment, chloroform-d, 600MHz -1.97 -1.63 T T o 9.18 - 27.61-I 5.5 T 4.5 4.0 5.0 3.5 3.0 2.5 T 1.0 1.5 1 0.5 0.0 (ppm)

Step by Step Solution

There are 3 Steps involved in it

1 Expert Approved Answer

Step: 1 Unlock blur-text-image

Question Has Been Solved by an Expert!

Get step-by-step solutions from verified subject matter experts

Step: 2 Unlock

Step: 3 Unlock

Students Have Also Explored These Related Chemical Engineering Questions!

From your IR spectrum explain what chemical bonds are present and absent in your unknown. Be specific. PLEASE ANSWER ALL QUESTIONS! Question one- three is based on the 1HMNR spectra found from the...

12. You've isolated a new molecule and alyva gave a formula of CH... You have ated on the options to the income shown below. (15) Using the NMR spectra collected on the sext page) no circle the...

As discussed in the "A Word About . . . NMR in Biology and Medicine" on page 368, MRI typically uses 1H NMR spectra of water in various tissues. What is the disadvantage of using 13C NMR spectra?...

3. Draw the mechanism (including electrophile formation) and product for the following INTRAMOLECULAR Friedel-Crafts reaction. Using the NMR spectra below, describe how your product is correct...

How would you distinguish among the compounds within each of the following sets using their NMR spectra? Explain carefully and explicitly what features of the NMR spectrum you would use. (a)...

A continuous stream of saturated liquid benzene (P=10 bar, T=178.6C) flows through an adiabatic throttling platc (i.e., oritice plate). The plate is essentially a barrier that contains a small hole...

6-3: Interpreting NMR Spectra - 2 Interpreting NMR spectra is a skill that often requires some amount of practice, which in tum. necessitates access to a collection of NMR spectra. Virtual Chemlab...

Compounds Selected: Chlorobutane, Ethyl Ether, KOH FTIR Conne IUPAC Nure ch Toid 00 WOO Cewe Monte " TH NMR UPAC Nase Solence Polar VP 120 THU 8 AR 251 2010 0:00 2 For this assignment, the target...

Interpreting NMR spectra is a skill that often requires some amount of practice, which, in turn, necessitates access to a collection of NMR spectra. Beyond Labz Organic Synthesis and Organic...

help me with all these please this is all question given Just answer eg 1H nmr d = 10 3. 21 15 H 14 UH 14 196 17 18 -N 19 11 H 10 HO... , 2N 11 H 19 G You are provided with a set of NMR data...

2. A wholesale nut company produces almond meal with daily total cost C which depends on the amount of almond meal produced that day in the following way: C(q)=2q-30q+200, where q is the amount of...

An 11-month-old child pushed on a window screen that gave way, allowing him to fall from the second story of his aunts house. The childs parents sued the screen maker. a. What product liability...

ast year, Kennedi purchased a fixed - rate, 1 0 - year bond at par that has a coupon rate of 4 . 2 percent. If the current market rate for this type and quality of bond is 4 . 5 percent, then she...

#10 Storage Performance: Mixed Methods Consider a spinning HDD with a random access time of 90ms and an effective transfer rate of 60MB/s. Now consider an SSD with a random access time of 100s and an...

Patients in the UK have historically been unable to choose their health care provider, but recent reforms have created options for patient choice.

If your plan is successful, what changes will occur? Who will make them happen?

Would you choose an indirect or direct pattern of organization to propose the idea? Why?