Question: Assignment 4 In this assignment you are provided information on an experiment and you are required to investigate and interpret the output which is provided

Assignment 4

In this assignment you are provided information on an experiment and you are required to investigate and interpret the output which is provided below.

Problem: Consider the three?variable central composite design shown in the table. 

RunOrderPtTypeBlocksTemperatureTimeCatalystConversion (%) y1Viscosity y2
111-1-1-17453.2
2111-1-15162.9
311-11-18853.4
41111-17062.6
511-1-117157.3
6111-119067.9
711-1116659.8
8111119767.8
9-11-1.68179007659.1
10-111.681793007965.9
11-110-1.6817908560
12-1101.68179309760.7
13-1100-1.681795557.4
14-11001.6817938163.2
15010008159.2
16010007560.4
17010007659.1
18010008360.6
19010008060.8
20010009158.9

 

Modified fromDesign and Analysis of Experiments (9th Edition) [Texidium version]. (2017). Retrieved from http://texidium.com

Part 1- Conversion percent

A partial Minitab output for the full model is shown below.

 

Model Summary

SR-sqR-sq(adj)R-sq(pred)
4.7166991.99%84.79%75.66%

 

 

Fits and Diagnostics for Unusual Observations

ObsConversion
% (y1)
FitResidStd
Resid
 
2091.0081.099.912.30R

R  Large residual

Analysis of Variance

SourceDFAdj SSAdj MSF-ValueP-Value
Model92555.73283.9712.760.000
  Linear3763.05254.3511.430.001
    Temperature114.4414.440.650.439
    Time1222.96222.9610.020.010
    Catalyst1525.64525.6423.630.001
  Square3601.30200.439.010.003
    Temperature*Temperature148.4748.472.180.171
    Time*Time1124.48124.485.600.040
    Catalyst*Catalyst1388.59388.5917.470.002
  2-Way Interaction31191.37397.1217.850.000
    Temperature*Time136.1236.121.620.231
    Temperature*Catalyst11035.121035.1246.530.000
    Time*Catalyst1120.13120.135.400.043
Error10222.4722.25  
  Lack-of-Fit556.4711.290.340.869
  Pure Error5166.0033.20  
Total192778.20   

 

Interpret the above output. As well as discussing factor significance you are expected to discuss the unusual residual and how it may (or may not) affect the overall analysis. Is there a specific recommendation that you would make?

The partial output for the reduced model is provided.

Model Summary

SR-sqR-sq(adj)R-sq(pred)
5.0585688.95%82.50%69.18%

 


 

 

Coded Coefficients

TermCoefSE CoefT-ValueP-ValueVIF
Constant79.591.7545.450.000 
Temperature1.031.370.750.4671.00
Time4.041.372.950.0121.00
Catalyst6.201.374.530.0011.00
Time*Time3.121.332.350.0361.01
Catalyst*Catalyst-5.011.33-3.780.0031.01
Temperature*Catalyst11.371.796.360.0001.00
Time*Catalyst-3.881.79-2.170.0511.00

Analysis of Variance

SourceDFAdj SSAdj MSF-ValueP-Value
Model72471.13353.0213.800.000
  Linear3763.05254.359.940.001
    Temperature114.4414.440.560.467
    Time1222.96222.968.710.012
    Catalyst1525.64525.6420.540.001
  Square2552.83276.4210.800.002
    Time*Time1141.78141.785.540.036
    Catalyst*Catalyst1365.42365.4214.280.003
  2-Way Interaction21155.25577.6222.570.000
    Temperature*Catalyst11035.121035.1240.450.000
    Time*Catalyst1120.13120.134.690.051
Error12307.0725.59  
  Lack-of-Fit7141.0720.150.610.736
  Pure Error5166.0033.20  
Total192778.20   

Assignment 4In this assignment you are provided information on an experiment and

Image transcription text

Residual Plots for Conversion (%) y1 Normal Probability Plot Versus Fits 10 90 Percent 50 Residual 10
10 50 70 90 Residual Fitted Value Histogram Versus Order 10 4.5 Frequency 3.0 Residual 1.5 -S -5.0
-2.5 0.0 2.5 5.0 7.5 10.0 12.5 2 4 6 10 12 14 16 18 20 Residual Observation Order

 

 

State (with justification) your proposed model equation for Conversion percent. 

Part 2

A reduced model for viscosity was developed in Minitab


 


 

Coded Coefficients

TermCoefSE CoefT-ValueP-ValueVIF
Constant59.9480.417143.650.000 
Temperature3.5830.3959.070.0001.00
Catalyst2.2300.3955.650.0001.00
Temperature*Temperature0.8230.3812.160.0461.00

 

Model Summary

SR-sqR-sq(adj)R-sq(pred)
1.4593388.14%85.91%63.02%
    

Analysis of Variance

SourceDFAdj SSAdj MSF-ValueP-Value
Model3253.20484.40139.630.000
  Linear2243.264121.63257.110.000
    Temperature1175.352175.35282.340.000
    Catalyst167.91267.91231.890.000
  Square19.9399.9394.670.046
    Temperature*Temperature19.9399.9394.670.046
Error1634.0742.130  
  Lack-of-Fit1130.4212.7663.780.077
  Pure Error53.6530.731  
Total19287.278   

 

Fits and Diagnostics for Unusual Observations

ObsViscosity
(y2)
FitResidStd Resid 
959.10056.2502.8502.98R
1065.90068.302-2.402-2.51R

R  Large residual

you are required to investigate and interpret the output which is provided

Image transcription text

Residual Plots for Viscosity (y2) Normal Probability Plot Versus Fits 3.0 1.5 Percent 50 Residual 10 -1.5
-3.0 4 SE 70 Residual Fitted Value Histogram Versus Order 3.0 1.5 Frequency Residual A -1.5 -3.0 -2 -1 2
2 4 10 12 14 16 18 20 Residual Observation Order

 

Comment on this model. What further action might you take based on the residuals?

Part 3

We are required to optimize the two responses.

Contour plots are as shown

 

below.Problem: Consider the three?variable central composite design shown in the table. RunOrderPtTypeBlocksTemperatureTimeCatalystConversion (%) y1Viscosity

Image transcription text

Contour Plots of Conversion (%) y1 Time*Temperature Catalyst*Temperature Hold Values Temperature
0 Time 0 Catalyst 61 0 -1- $7 . 47 -1 0 1 Catalyst* Time -1 1

 

y2111-1-1-17453.22111-1-15162.9311-11-18853.441111-17062.6511-1-117157.36111-119067.9711-1116659.88111119767.89-11-1.68179007659.110-111.681793007965.911-110-1.681790856012-1101.68179309760.713-1100-1.681795557.414-11001.6817938163.215010008159.216010007560.417010007659.118010008360.619010008060.820010009158.9 Modified fromDesign and Analysis of Experiments (9th Edition) [Texidium version]. (2017). Retrieved

Image transcription text

Contour Plot of Viscosity y2 vs Catalyst, Temperature 1.5 62.5 65.9 69.3 59.1 1.0 0.5 67.6 Catalyst 0.0
$5.7 -0.5 -1.0 04 2 -1.5 54.0 57.4 60.8 -1.5 -1.0 -0.5 0.0 0.5 1.0 1.5 Temperature

 

 On the assumption that we want to maximize conversion percent while maintaining viscosity between 55 and 60 where would you propose that the inputs be set? Clearly justify your response on the basis of the contour plots.

 

Your manager has decided to change the viscosity requirement to be a target of 65. Interpret the response optimizer output below

from http://texidium.comPart 1- Conversion percentA partial Minitab output for the full model is

Image transcription text

Optimal Temperat Time Catalyst D: 1.000 High 1.6818 1.6818 1.6318 Cur [1.0984] [1.6818] [0.0552] Low
-1.6818 -1.6818 -1.6818 Composite Desirability D: 1.000 Viscosit Targ: 65.0 y = 65.0 d = 1.0000 Conversi
Maximum y = 97.0 d = 1.0000

 

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