Estimate the boiling points from the plots and identify the two components in your unknown (be sure to note which unknown you used) a. Possible unknowns :Hexane, Cyclohexane, Heptane, Toluene and Ethylbenzene Write a sentence or two describing how the plot was used to identify your unknown On each GC-MS spectrum label the peaks that correspond to the proposed components in your unknown sample and record the retention times for each peak. Include you and your partner's GC-FID spectra in the lab report FID1 0.572 0.619 15000000 Fractional Distillation 1.5mL 10000000 5000000 9211 1.0 1.5 20 0.5 2.5 min Unit Name Mark SV FID1 Peak# Ret. Time Area Height 1 0.572 254392849 181359103 2 0.819 25004857 17177955 3 1.129 1239 911 4 1.166 1263 863 Total 279400208 198538831 Conc. 0.000 0.000 0.000 0.000 100000 0.579 FID1 1880 T:198 75000- Fractional distillation 5.5mL 50000 25000- 1.307 0.680 0.5 1.0 1.5 2.0 2.5 min Unit Name FID1 Peak# Ret. Time Area Height 0.579 167136 97447 2 0.680 7741 3501 3 0.883 380558722 113021629 4 1.140 114757 91738 5 1.176 134738 103948 6 1.307 16373 11903 Total 380999467 113330166 0 CON Conc 0.000 0.000 0.000 0.000 0.000 0.000 Mark V V SV T TV T FIDT 0.575 0.870 Simple distillation 5.5mL 30000000 20000000 10000000 0.528 1193 1.305 0.5 1.0 1.5 2.0 2.5 min Unit Name FID1 Peak# Ret. Time Area Height 1 0.528 1394 1075 2 0.575 55619716 35631291 3 0.870 278024401 95824186 4 1.137 59781 48447 5 1.173 71578 52213 6 1.305 8573 6187 Total 333785444 131563400 Conc. 0.000 0.000 0.000 0.000 0.000 0.000 Mark V SV SV T TV T 50000000 0.573 0.838 FID1 40000000 30000000 Simple distillation 1.5mL 20000000 10000000 0.5 1.0 1.5 2.0 2.5 min Unit Mark Name FID1 Peak# Ret. Time Area Height 1 0.573 195346801 137681061 - 2 0.838 93016925 49214690 3 1.132 11302 8389 4 1.168 12550 8769 5 1.300 1510 1037 Total 288389087 186913946 Conc 0.000 0.000 0.000 0.000 0.000 isinin Simple Distillation Data 2 Volume (ml) Temperature (C) 0.5 75C 1 85 C 1.5 90C 94 C 2.5 3 100C 3.5 4 930 4.5 980 100C 5.5 102 C Fractional Distillation Volume Temperature (mL) (C) 0.5 : 6C 1 69C 1.5 : 20C 2 22C 2.5 68C 3 03 3.5 100C 4: 1050 4.5 10C 5 106oc. 5.5 108C in win iniinin | | | 92 DC in un in Estimate the boiling points from the plots and identify the two components in your unknown (be sure to note which unknown you used) a. Possible unknowns :Hexane, Cyclohexane, Heptane, Toluene and Ethylbenzene Write a sentence or two describing how the plot was used to identify your unknown On each GC-MS spectrum label the peaks that correspond to the proposed components in your unknown sample and record the retention times for each peak. Include you and your partner's GC-FID spectra in the lab report FID1 0.572 0.619 15000000 Fractional Distillation 1.5mL 10000000 5000000 9211 1.0 1.5 20 0.5 2.5 min Unit Name Mark SV FID1 Peak# Ret. Time Area Height 1 0.572 254392849 181359103 2 0.819 25004857 17177955 3 1.129 1239 911 4 1.166 1263 863 Total 279400208 198538831 Conc. 0.000 0.000 0.000 0.000 100000 0.579 FID1 1880 T:198 75000- Fractional distillation 5.5mL 50000 25000- 1.307 0.680 0.5 1.0 1.5 2.0 2.5 min Unit Name FID1 Peak# Ret. Time Area Height 0.579 167136 97447 2 0.680 7741 3501 3 0.883 380558722 113021629 4 1.140 114757 91738 5 1.176 134738 103948 6 1.307 16373 11903 Total 380999467 113330166 0 CON Conc 0.000 0.000 0.000 0.000 0.000 0.000 Mark V V SV T TV T FIDT 0.575 0.870 Simple distillation 5.5mL 30000000 20000000 10000000 0.528 1193 1.305 0.5 1.0 1.5 2.0 2.5 min Unit Name FID1 Peak# Ret. Time Area Height 1 0.528 1394 1075 2 0.575 55619716 35631291 3 0.870 278024401 95824186 4 1.137 59781 48447 5 1.173 71578 52213 6 1.305 8573 6187 Total 333785444 131563400 Conc. 0.000 0.000 0.000 0.000 0.000 0.000 Mark V SV SV T TV T 50000000 0.573 0.838 FID1 40000000 30000000 Simple distillation 1.5mL 20000000 10000000 0.5 1.0 1.5 2.0 2.5 min Unit Mark Name FID1 Peak# Ret. Time Area Height 1 0.573 195346801 137681061 - 2 0.838 93016925 49214690 3 1.132 11302 8389 4 1.168 12550 8769 5 1.300 1510 1037 Total 288389087 186913946 Conc 0.000 0.000 0.000 0.000 0.000 isinin Simple Distillation Data 2 Volume (ml) Temperature (C) 0.5 75C 1 85 C 1.5 90C 94 C 2.5 3 100C 3.5 4 930 4.5 980 100C 5.5 102 C Fractional Distillation Volume Temperature (mL) (C) 0.5 : 6C 1 69C 1.5 : 20C 2 22C 2.5 68C 3 03 3.5 100C 4: 1050 4.5 10C 5 106oc. 5.5 108C in win iniinin | | | 92 DC in un in