Question: I need help determining my compound using the spectra below. A general idea for the compound is written in the first image. The Experiment: In



The Experiment: In this experiment you will acylate an unknown aromatic compound using acetyl chloride and aluminum chloride. The unknown will be one of the following compounds: toluene ethylbenzene 0-xylene (1,2-dimethylbenzene) mesitylene (1,3,5-trimethylbenzene) m-xylene (1,3-dimetylbenzene) cumene (isopropylbenzene) p-xylene (1,4-dimethylbenzene) p-cymene (1-isopropyl-4-methylbenzene) anisole (methoxybenzene) tert-butylbenzene Each reaction gives predominantly one substituted acetophenone product, which you will purify by vacuum distillation. The structure of the product will be determined by IR and H and 13C NMR, allowing you to determine which of the above aromatic compounds you started with. R AICI CH,CI2 Unknown Acetyl Chloride Substituted Acetophenone 12.022 brez 1.00 021 0.121 003 0.01 all 13 12 10 6 S PPM samer oferinte.closcanes iz CamScanner Y Units 0.6 0.7 0.3 0.4 0.5 0.8 0.9 1.0 3500 cs Scannessowith scom Sca,scoer 3000 X Units 2000 1676.39 1609.74 1565.84 1500 1352.97 1444.08 1379.15 1293.50 - 1232.57 - 1252.193 1000 1145.20- 1035.41 1058.02 965.94 915.77 812.59 675.62 584.07-801.00 547.84 - 500 433.90 dom 247.00 198.00 141.457 - 138.54 132.710 Dam Scanner - 134.680 125.922 130.124 -45254 28.404 21.601 20.631 -0.001 -5.500 150 PPM The Experiment: In this experiment you will acylate an unknown aromatic compound using acetyl chloride and aluminum chloride. The unknown will be one of the following compounds: toluene ethylbenzene 0-xylene (1,2-dimethylbenzene) mesitylene (1,3,5-trimethylbenzene) m-xylene (1,3-dimetylbenzene) cumene (isopropylbenzene) p-xylene (1,4-dimethylbenzene) p-cymene (1-isopropyl-4-methylbenzene) anisole (methoxybenzene) tert-butylbenzene Each reaction gives predominantly one substituted acetophenone product, which you will purify by vacuum distillation. The structure of the product will be determined by IR and H and 13C NMR, allowing you to determine which of the above aromatic compounds you started with. R AICI CH,CI2 Unknown Acetyl Chloride Substituted Acetophenone 12.022 brez 1.00 021 0.121 003 0.01 all 13 12 10 6 S PPM samer oferinte.closcanes iz CamScanner Y Units 0.6 0.7 0.3 0.4 0.5 0.8 0.9 1.0 3500 cs Scannessowith scom Sca,scoer 3000 X Units 2000 1676.39 1609.74 1565.84 1500 1352.97 1444.08 1379.15 1293.50 - 1232.57 - 1252.193 1000 1145.20- 1035.41 1058.02 965.94 915.77 812.59 675.62 584.07-801.00 547.84 - 500 433.90 dom 247.00 198.00 141.457 - 138.54 132.710 Dam Scanner - 134.680 125.922 130.124 -45254 28.404 21.601 20.631 -0.001 -5.500 150 PPM
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