Question: Please show all necessary work. The procedure is also added. Will rate, thank you. Chemistry 3232 Organic Chemistry Experiment 1: The Diels-Alder Reaction; Synthesis of
Please show all necessary work. The procedure is also added.
Will rate, thank you.


Chemistry 3232 Organic Chemistry Experiment 1: The Diels-Alder Reaction; Synthesis of 9,10-Dihydroanthracene- Pre-lab Exercises 1. Write out the chemical equation for the Diels-Alder reaction of anthracene with maleic anhydride showing structures of the reactants and the product. 2. Fill in the table of reactants and solvents. Calculate molecular weights and mmol of 3. Which reagent is limiting? 4. Calculate the theoretical yield in mmol and mg. Show your work. Procedure 1. Weigh and place 80mg of anthracene and 40mg of maleic anhydride in a small rb flask located in your microscale kit. Add 1.0mL of xylene, a boiling stone, and equip the flask with an air condenser. 2. Set up a reflux apparatus using a hot plate. Reflux the mixture vigorously for 60 minutes. Allow the mixture to cool to room temperature, and then place it in an ice bath for 10 minutes. 3. Collect the crystals by vacuum filtration using the Hirsch funnel in your microscale kit. Be sure to scrape out solid product that may stick to the inner walls of the condenser. Wash the filtered solid with two small (
Step by Step Solution
There are 3 Steps involved in it
Get step-by-step solutions from verified subject matter experts
