Question: Procedure and Observations PART A Synthesis Added 2 . 5 ml of methanol ( 3 2 . 0 4 g / mol ) , 0
Procedure and Observations
PART A Synthesis
Added ml of methanol gmolg of camphor gmol and a stir rod to a mL round bottom flask RBF clamped to a retort stand on top of an ice bath. Stir until dissolved so the solution is clear and transparent. Keeping the ice water bath, add g of NaBH gmol over minutes while stirring and only adding a small tip while waiting for the bubbles to subside before adding again. Once all the NaBH is added, remove it from the ice bath and continue to stir until most of the bubbling has stopped and the reaction is at room temperature. Install a consider and place the flask in a deg C water bath while continuing to stir and maintain the hot plate between seven and six settings. Allow the mixture to reflux for minutes; vapours should condense and drip back into the flask refluxing Remove from bath and allow to cool to room temperature.
PART B Isolation and Purification
Once the mixture has reached room temperature, add mL of icecold deionized DI water gmol to the flask. Filter the opaque white precipitate that forms through a Bchner funnel and vacuum dry for a minimum of five minutes. Rinse the RBF with cold DI water to remove any remaining precipitate into the Bchner funnel. Once dry, transfer the white solid to a mL Erlenmeyer flask using weigh paper, and add mL of diethyl ether gmol to dissolve the precipitate fully. Crush the precipitate, if needed, to get it to dissolve andor add mL more to dissolve the precipitate fully. The solution using anhydrous magnesium sulfate MgSO and filter, using filter paper, into a clean mL RBF Rinse the Erlenmeyer flask with ~ mL of diethyl ether and pour into the funnel to filter out the MgSO Rinse one more time, then use a rototap to remove the solvent. Wait for the ether to evaporate, then use gas to dry even more, and proceed to weigh the yield fully.
QUESTION: Show the Full reaction mechanism with ALL arrow pushing, explain the reaction mechanism and connect the procedure steps to the chemistry, explaining the reaction with proper chemical terminology without repeating the procedure.
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