Question: Show your work on each spectrum Show your work calculating your potential molecular formulas using Mass Spec Clearly label IR stretches and their corresponding functional
- Show your work on each spectrum
- Show your work calculating your potential molecular formulas using Mass Spec
- Clearly label IR stretches and their corresponding functional groups
- Clearly label all NMR resonances, assigning a proton or carbon to each peak
- Walk me through your logic in paragraph form
- Identify other possible compounds, but clearly state why they are eliminated as possible answers upon further review
- Draw your final structure
LETI1 2 900 TO T&TT 16 1379 02 1465 47 152379 GE 26 TB 856 64 96 TGBZ DEZ 1952 TOTTE 66 EGEE 4 1621 BE AVENURSERII 095 DOST DO 001 Unknown B PH INDEX 1 HEIGHT 48. FREQUENCY 1228.9 1217.1 1210.2 602.8 2.435 59.7 7.2 4 5 1.206 1.204 1.106 550. 512.5 587.7 580.a 24.2 10.8 35.2 99.1 11 Seaple Name Unknown DATA 0011acted on: mr-veres Archive directory /home/alkup./var sys/data Unknown_O_20131195_02 FidFile slabe1_01 Pulse Sevence: PILOTON (2) Solvent: cdc1a Data collected on Nov 5 2018 Temp. 24.00 217.1K Sample 20. Operatori Walup Relax. delay 1.0DD SEG Pulse 45.0 degrees Acq- tine 2.045 30 Vidin 8012.8 HZ 64 repetitions OBSERVE WL, 489.7070810 MM DATA PRDOESNO FT 12 32768 Total ttas 3 min 15 sec 557.0 50 a 553.4 1.162 1.140 1.130 1.121 1.10 7.5 25.5 13 15 1.078 2.1 537.8 591.4 427.2 942.1 334.0 17 1a 0.ass 18.8 4.7 21.2 13.0 144.0 0.670 0.655 VVV 15. 12 10 2 D ppm PPM INDEX 1 2 HEIGHT 48.3 FREQUENCY 1223.3 1217.1 1210.2 801. 602.3 7.2 6.8 10.3 1.109 1.18 Bangle Mans Unknown Data Collected on: ner- p500 Archive directory: Thone alapversys/data Sangle directory: Unknown__20161101_02 FioF1101 pilab1_01 Pulse Sequence: PROTON (S2pul) Solvent: cdc13 Data collected on Nov 5 2018 Temp. 24.0 C 297.1 K Sample 020, Operator: maikup Relax. delay 1.990 sec Pulse 45.0 degrees Acg. time 2.045 Gec Width 4012, WE 60 repetitions OBSERVE N1, 493.7070914 Miz DATA PROCESSING FT size 32700 Total tine a min 15 sec 592.5 587.7 sa. 574.0 567.6 560. 553.4 545.6 537.8 1.170 1.152 1.14 1.186 1.123 1.107 10 11 12 13 15 16 17 18 15 20 1.00 38.8 30.1 16.6 4.7 427.2 342.1 1.070 1.06 0.85$ 0.6BE B3.0 144.0 327.5 0.655 65.8 2.6 2.4 2.2 2.0 1.6 1.4 87.00 1.2 1.0 0.8 ppm HETGHT 22.7 INDEX 1 2 3 4 s FREDUENCY PPM 9740.2 77.505 77.255 3673 76.997 5238.5 41.687 4500. as.313 2477.0 13.71 1710.3 13.00 20.4 102.1 112. 102.0 7 Barpte Nanti Unknown Data Collected as ner-p-500 Archive directory: home aloup/vir sys/data Sample directory Unknown_1_20161109_01 FidFilet pelabai_01 Pulse Sequence: CARBON (szpul) Solvent de 13 Data collected on Nov 5 2018 Temp. 24.0 6 / 297.1 K Sample 020, Operator: walkup Relax. dolny 1.690 e Pulse 45.0 degrees Ace. tiek 1.025 sec width 31250.0 MZ 512 repetition OBSERVE C13, 125.6715516 MHZ DECOUPLE H1, 489.7895683 MHZ Power 42 dB continuously on WALT2-18 modulated DATA PROCESSING Line broadening 0.5 Hz FT 126 65536 Total time 17 ain 220 200 180 160 140 120 100 80 60 40 20 0 ppn Unknown Mass of molecular ion: 731 100- 80- 60 Relative Intensity 40 20- ottir 10 20 30 40 50 60 70 80 90 m/z Source Temperature: 280 C Sample Temperature: 150 C RESERVOIR, 75 eV
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