Question: Structure? 2.2 2.0 1.8 1.6 1.4 1.0 1.2 1 ppm COSY 600 MHz ppm 2.4 1.0 - 1.0 1.2- 1.2 1.4 - 1.4 F1 1.6

Structure? 2.2 2.0 1.8 1.6 1.4 1.0 1.2 1 ppm COSY 600Structure?

2.2 2.0 1.8 1.6 1.4 1.0 1.2 1 ppm COSY 600 MHz ppm 2.4 1.0 - 1.0 1.2- 1.2 1.4 - 1.4 F1 1.6 - 1.6 1.8 1.8 2.0 - -2.0 2.2- -2.2 F2 HMQC 600 MHz ppm w 15 - 15 20 -20 25 -25 F1 30 -30 . 35 -35 40 -40 45 -45 1 2.4 2.2 2.0 1.8 1.4 1 1.0 1.2 ppm 1.6 F2

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