Question: For simplicity, let s assume ethanol is easily separated from the products such that a saturated liquid mixture of 6 5 mol % ethyl acetate,

For simplicity, lets assume ethanol is easily separated from the products such that a saturated
liquid mixture of 65 mol% ethyl acetate, with balance acetic acid, needs to be distilled to produce
a distillate of 95 mol% ethyl acetate and a bottoms of 10 mol% ethyl acetate. Assume a total
condenser and partial reboiler.
The vapor-liquid equilibrium data are given as mole fractions of ethyl acetate and plotted as
shown:
Liquid, x Vapor, y
0.0000.000
0.1630.473
0.3170.689
0.5800.893
0.7310.949
0.9030.979
0.9300.987
1.0001.000
In answering the following questions, please provide all number of stages to one decimal place.
Note you can use the lever rule to estimate fractional stages. You may find it helpful to copy the
graph above for each sub-part of the problem and draw the lines onto the graph. Also, note that a
partial reboiler is an equilibrium stage but not considered a tray in the column.
a. What is the minimum number of equilibrium stages needed for this system?
b. What is the minimum reflux ratio (Rmin) needed for this separation to occur? Note that at
minimum reflux, the number of stages goes to infinity. What is the boilup ratio at this
reflux?
c. Let R =1.5 Rmin . How many equilibrium stages are required for this separation? What is
the optimal feed stage

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