Question: Analyse the compound as complete as possible IR 1H 13C DEPT COSY HMBC HMQC Molecule 2A 100.0. 95 90 85 80 446 87 75

Analyse the compound as complete as possible IR 1H 13C DEPT COSY HMBC HMQC Molecule 2A 100.0. 95 90 85 80 446 87 75 70 65 60 1405 26 55 50 %T sp03 08 3115.17 45 1109 86 40 860.7 35 801.01 878 70 30 1806 92 1428.35 25 1541 27 716.53 20 15 1351.06 10 1693.47 129261 1280.06 0.0 4000.0 3600 3200 2800 2400 2000 1800 1600 1400 1200 1000 800 600 400.0 cm-1 PS1 13C NMR BRKER 1.40 210 200 190 170 160 165.73 149.90 136.27 130.61 123.60 39,86 39.65 -39.44 39.23 -39.02 38.81 38.60 PS1 11 1 "D: \NMREXP \Wan Mohd Khairul" nmr PS1 14 1 "D: \NMREXP \Wan Mohd Khairul" nmr PS1 13 1 "D: \NMREXP\Wan Mohd Khairul" nmr PS1 12 1 "D: \NMREXP \Wan Mohd Khairul" nmr Scale : 1.7611 PS1 11 "D: \NMREXP \Wan Mohd Khairul" nmr Scale : 1.8492 200 150 100 50 [ppm] (991.1 008 09 PS1 H NMR BRKER Current Data Parameters PS1 NAME 10 1 EX PNO PROCNO F2 - Acquisition Parame ters Da te Time INSTRUM 20150 304 10.50 spect 5 mm PABBO BB- zg30 65536 DMSO 300 2 PROBHD PULPROG TD SOLVENT NS DS SWH 8223. 685 Hz 0. 125483 H z 3.9845889 sec 40.3 60.800 usec 6.50 usec 300.0 K 1.00000000 sec FI DRES AQ RG DW DE TE D1 TDO 1 -------- CHANNEL f1 - - 8.5 8.4 8.3 8.2 8.1 NUC1 P1 1H 14.20 usec ppm PL1 -1.00 dB PL1W SFO1 12.33288288 W 400.1124708 MHz F2 - Processing parameters 32768 400.1100000 MH2 SI SF WDW EM SSB LB 0.30 Hz GB PC 1.00 10.5 10.0 9.5 9.0 8.5 8.0 7.5 7.0 6.5 6.0 5.5 5.0 4.5 4.0 3.5 3.0 2.5 2.0 1.5 1.0 0.5 0.0 ppm 8.114 - 4.985 OLSZ- PS1 COSY BRUKER ppm Current Data Paranetera 15 PROCO 12 - Aequiaition Paraneter 20150s04 19.30 apect PROBED 5 m FA BO n- coaypat 204 F0.0 Pate Time IMSTREM F0.5 PULPROG SOLVENT 40 F1.0 S 3649.635 lz 1, 78204 RE 0.2805760 FIDRES F1.5 aec 36 137.000 usec RG 6.50 uec 300.0 K 0.00000300 an DE TE do F2.0 c 1.39800894 sec 0.0000040D see D1 D16 ind 0.00020000 see O sec F2.5 128 6.00000300 sec STior dborig philoop tiloop F3.0 sroi 400.1123566 Ml: PO 14.20 usec 14.20 unee -1.00000000w 3.5 GAM |1) GPEI SIME.100 10.00 P16 1000.00 usec F4.0 ri - Aequisition paraneter 128 400.1124 M TIDRES 28.512774 H: F4.5 9.122 ppm r2 - Procening paranetera 1024 400.110000D MRE STE -5.0 SI SINE 5.5 1.40 F6.0 - Proceasing paranetera 1024 gr 400.1100000 M: ST SINE F6.5 O Rz E7.0 7.5 F8.0 -8.5 F9.0 F9.5 9.5 9.0 8.5 8.0 7.5 7.0 6.5 6.0 5.5 5.0 4.5 4.0 3.5 3.0 2.5 2.0 1.5 1.0 0.5 0.0 ppm PS1 HMBC -120 -130 9.5 9.0 8.5 8.0 7.0 6.5 6.0 5,5 5.0 4.5 4.0 3.5 3.0 2.5 2.0 ppm PS1 HMQC 120 130 140 12 11 10 5 4 8 ppm

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