Question: instrumental methods analysis wave length =0.165 2 theta (24.7) (34) (36) X-Ray Diffraction (XRD) is a method used widely in the determination of a crystal

instrumental methods analysis

wave length =0.165

2 theta (24.7) (34) (36)

X-Ray Diffraction (XRD) is a method used widely in the determination of a crystal structure of a compound. [1000 words] i) Each student will be provided with a XRD Spectrum. Student should make a complete analysis of the spectrum, with suitable justification. [15] ii) Discuss the benefits and limitations of XRD technique in Chemical Analysis [10] 3 = 0.165 Intensity (a.u) (012) () (011) (104) (20) 20 247 30 34 36

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