Question: please answer questions 1 and 2 Create a data table. Record the mass of each components separated from the drug Calculate the % Composition of




Create a data table. Record the mass of each components separated from the drug Calculate the % Composition of the substances in the drug. Identify the unknown component in the drug. Explain briefly how you reach the result. Determining the Unknown Substance: Melting Point (m.p.) Determining by physical property of melting point Pure substances will fully melt more closely to its reported melting temp. The more impure the mp becomes broader (substances starts melting earlier and finishes melting at a higher temp). Mp also becomes much lower than reported mp also Substance Acetanilide Phenacetin Melting point (C) 114 135 "Use slide show at this point to see animations add Sucrose does not dissolve Panacetin 3.000g DCM Gravity Filter Filtrate - Organic Soln Dry Sucrose 320g Add NaHCO, Mix Organic Soln 2 sep. Portions Rd Separatory Funnel Separate Vacuum Filter Video Link Dried Aspirin -1.1868 Aqueous Layer Organic Layer Heat - Organic Layer Isolated Unknown-1.510 8 Recrystallize Required 124 mL of H,0 to dissolve Melting point Melting point was 130 C Watch Meltetemp Video, Isolated Porified Unknown1.4218
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