Please help fill out the chart and if you can explain how you got your answers. thank you!

Chemicals land equinmentl Table: "Literature values can be reliably obtained from "Wikipedia" (internet), but should be checked with other reliable sources such as Aldrich.com or FisherSci.com. Solubility implies often >1g/100mL. ** The moles of solvent used and moles of any catalyst used are not important to stoichiometry. *s* The literature BP is recorded for liquids; the literature MP is recorded for solids. Procedure: Touchette, K. M. Journal of Chemical Education 2006, 83 (6), 929-930. Part 1: Synthesis of a drug-like tertiary amide by reductive amination Reductive Amination: In a tared beaker ( 100mL of greater), combine 400mg paratoluidine and 570mg ortho-vanillin. Note the color of the two starting materials. Crush and mix the solids together with a spatula until a color change is observed and the solids melt together. Continue until the mixture becomes a dry powder and then transfer approximately 50mg of this solid to a labeled test tube to save for IR analysis. To the remaining imine, add 7.5mL95%EtOH (the imine will only partially dissolve). Carefully add 150mgNaBH4 in portions so that the bubbling is constant, but not too vigorous. Occasionally swirl the mixture until no more bubbling occurs and the solution is homogeneous (it may be necessary to break up some of the small pieces of imine and/or NaBH4 with a spatula). Note any change in color. To the clear solution, add 1.1mL acetic acid and 1.1mL acetic anhydride, in that order. Gently warm the resulting solution in a hot water bath with swirling for 5-10 minutes. Remove the product mixture from the heat and cool to room temperature. Work-up: Add 20mL of deionized water to the solution. A white solid should precipitate. Filter and collect the solid by vacuum filtration. Allow the solid to dry until the end of the lab period and obtain a yield. Analysis: Take an IR spectrum of the imine intermediate you saved from the first step in Part 1 and note its color in your notebook. Also record IR of the final product. Normally a melting point range would be recorded, but the product will not have sufficient time to dry thoroughly to get a useful MP range (might still be wet with trace amounts of solvent, which dramatically reduce the MP range for this compound)