Question: Q . 2 . A distillation column is to be designed to separate a mixture of acetone water having a maximum feed rate of 1

Q.2. A distillation column is to be designed to separate a mixture of acetone water having a maximum
feed rate of 15000kgh. The feed contains 4% acetone and the top product contains 95% acetone by
weight. The bottom product is essentially water. Consider the turndown ratio as 75%, no of real trays
18, the slope of enriching section operating line as 0.6, and, the slope of rectifing section operating
line as 4.5. Estimate the following considering a single-pass cross-flow tray pattern. Tray spacing =600
mm, hole/active area =0.08.
a) Flooding velocity
b) Column diameter ({:Dc)
c) Downcomer area (Ad), net area (An), active area (Aa), perforated area (A0), hole area (An),
d) weir length ({:Iw), weir height (hw), hole diameter (hd), and number of holes.
e) Minimum vapor velocity at turn down ratio and for weeping and entrainment
f) Total pressure drops in mm liquid
g) Downcomer liquid backup.
h) Residence time
and comment on your answers wherever required.
Given data:
Base tempt =100C, Top plate tempt =59C
Bottom plate: =0.7kgm3,l=960kgm3,L=60*10-3Nm
Top plate: v=2.15kgm3,L=760kgm3,L=25*10-3Nm
l=0.35*10-3Nsm2,V=10*10-6Nsm2,Dl=4.8*10-9m2sA column is to be designed to separate a mixture of ethylbenzene and styrene. The feed will contain 0.5mol fraction styrene, and a styrene purity of 99.5% is required, with a recovery of 85%. Estimate the number of equilibrium stages required at a reflux ratio of 8. Maximum column bottom pressure 0.20 bar. Formula/Expressions: ud 'OOL (AAIAA)
 Q.2. A distillation column is to be designed to separate a

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