Question 4: Fractional distillation is performed when two or more miscible compounds have a boiling point...

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Question 4: Fractional distillation is performed when two or more miscible compounds have a boiling point difference (A bp) less than 40 C. 2-Methylpentane and cyclohexane boil at 62 C and 80.7 C, respectively. Given gas chromatography (GC) data from your instructor, calculate the percent composition of each compound in Frxn 1 and Frxn 2. (X% 2-methylpentane: X% cyclohexane) [Note: Area = h width at h] Frxn 1 Peak 1 (2-Methylpentane) Peak 2 (Cyclohexane) Frxn 2 Peak 1 (2-Methylpentane) Peak 2 (Cyclohexane) Peak Height (h) mm mm Peak Height (h) mm mm Peak Width at Half Height mm mm Peak Width at Half Height mm mm Data File C:\Chem32\1\Data\ZJP2022 Sample Name: M8 DB 1 www Acq. Operator : SYSTEM Acq. Instrument : 7890A GC Injection Date Sequence File Method Last changed PA 40000 30000 20000 10000 0 ================: 1 2 3 4 5 FID1 A, Front Signal (053F5301.D) Totals : : 9/28/2022 8:50:12 PM 0.25 0.5 2022-09-28 17-44-43\053F5301. D CHE.231L.1 m@8? Inj Volume 0.1 ul : C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\ZJP2022.S : C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\ZJP2022.M (Sequence Method) : 9/28/2022 5:44:43 PM by SYSTEM Signal 1: FID1 A, Front Signal Peak RetTime Type Width # [min] [min] ||----| 0.777 BB 0.835 BB 0.912 BB S 0.948 BV T 1.315 BB S ======================= =================== 1920 Signal 1.0000 1.0000 Area Percent Report Area [pA*s] 0.777 0.835 Sorted By Multiplier : Dilution. : Do not use Multiplier & Dilution Factor with ISTDS 0.75 7890A GC 9/28/2022 8:52:12 PM SYSTEM =================================================== 0:912 Height [PA] 5.96839e4 6.64521e4 0.948 Seq. Line : 53 Location : 53 1 Inj: 7.99e-3 35.09433 73.25616 0.05880 0.0108 10.47289 15.99453 0.01755 0.0117 3.43577e4 4.72489e4 57.56605 0.0115 158.73891 223.91490 0.26597 0.0203 2.51219e4 1.88901e4 42.09164 *** End of Report *** Area 8 9.26.2022 GC Data For Exp. III Fractional Distillation 1.25 -1.315 1.5 -2-Methylpentane Cyclohexane =================== Page 1.75 1 of 1 m Data File C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\054F5401. D. Sample Name: M8_DB_2 ========== Acq. Operator : SYSTEM Acq. Instrument: 7890A GC Injection Date. : 9/28/2022 8:53:43 PM Sequence File Method Last changed pA 25000 20000 15000 10000 5000 0 Seq. Line : 54 Location : 54 Inj: 1 Inj Volume : 2022-09-28 17-44-43\ZJP2022.S : C:\Chem32\1\Data\ZJP2022 : C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\ZJP2022.M (Sequence Method) : 9/28/2022 5:44:43 PM by SYSTEM FID1 A, Front Signal (054F5401.D) Sorted By Multiplier Dilution 1 2 3 4 5 =================================== 0.25 ====================================== Totals : 0.5 : ============== Signal 1: FID1 A, Front Signal Peak RetTime Type Width # [min] ||-- 0.782 BB 8.75e-3 0.835 BB 0.910 BBS 0.947 BV T 1.323 BBS Signal 1.0000 1.0000 Area Percent Report Area [min] [pA*s] 429 0.782 0.835 : Do not use Multiplier & Dilution Factor with ISTDS 0.75 7890A GC 9/28/2022 8:55:43 PM SYSTEM 0.910 Height [PA] 5.89955e4 5.34101e4 $0.947 ================ 13 s 2 m === 1.77066 3.25276 0.00300 0.0111 2.45555 3.64279 0.00416 0.0118 1.96600e4 2.67821e4 33.32452 0.0120 111.55967 147.61584 0.18910 0.0229 3.92198e4 2.64735e4 66.47922 End of Report *** 0.1 ====================== Area 8 1.25 323 ======================== 1.5 Page 1.75 1 of 1 min Data File C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\055F5501. D Sample Name: M8_Tanvi_1 Acq. Operator : SYSTEM Acq. Instrument : 7890A GC Injection Date: Sequence File Method Last changed PA 35000 30000 25000 20000 15000 10000 5000 0 =========== 1 2 3 4 5 ================== : 9/28/2022 8:57:15 PM FID1 A, Front Signal (055F5501.D) 0.780 BB 0.833 BB Totals : 0.25 : C:\Chem32\1\Data\ZJP2022 : C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\ZJP2022.M (Sequence Method) : 9/28/2022 5:44:43 PM by SYSTEM 0.909 BB S 0.945 BB T 1.305 BB S Signal 1: FID1 A, Front Signal Peak RetTime Type # [min] ----| 0.5 Width [min] | Sorted By : Multiplier : Dilution : Do not use Multiplier & Dilution Factor with ISTDS. Area Percent Report Signal 1.0000 1.0000 Inj Volume 0.1 l 2022-09-28 17-44-43\ZJP2022.S 0.780 0.833 0.75 Area [pA*s] ========================= 0.909 Height [pA] 7890A GC 9/28/2022 8:59:15 PM SYSTEM Seq. Line : 55 Location : 55 Inj: 1 3.99095e4 4.55234e4 0.945 9.46e-3 1.11849 1.84932 0.00280 7.84525 11.69148 0.01966 0.0102 0.0123 2.72068e4 3.50337e4 68.17138 0.0116 121.41135 168.12975 0.30422 0.0190 1.25723e4 1.03080e4 31.50194 ***End of Report *** Area 8 1.25 1.305 ================ ================ ============ ============= 1.5 Page 1.75 1 of 1 min Data File C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\056F5601. D Sample Name: M8_Tanvi_2 Acq. Operator : SYSTEM Acq. Instrument: 7890A GC Injection Date Seq. Line : 56 Location : 56 Inj 1 Inj Volume: 0.1 pl : C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\2JP2022.S Sequence File Method. Last changed : C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\ZJP2022.M (Sequence Method) : 9/28/2022 5:44:43 PM by SYSTEM FID1 A, Front Signal (056F5601.D) 25000 PA 20000 15000 10000 5000 1 2 3 0 4 5 : 9/28/2022 9:00:46 PM 0,25 Totals : 0.5 : : Signal 1: FID1 A, Front Signal Peak RetTime Type Width # [min] [min] ==================== Area Percent Report ======== Sorted By Multiplier Dilution : Do not use Multiplier & Dilution Factor with ISTDS Signal 1.0000 1.0000 0.75 Area [pA*s] 0.835 Height [pA]: 7890A GC 9/28/2022 9:02:46 PM SYSTEM -0:910 5.89015e4 5.33811e4 0.835 BB 0.910 BB S 0.948 BV T 0.0112 2.52255 3.68258 0.00428 0.0119 2.09005e4 2.81609e4 35.48378 0.0121 128.53427 168.70262 0.21822 1.002 VB T 0.0134 1.28819 1.59166 0.00219 1.323 BB S 0.0224 3.78686e4 2.50462e4 64.29153 0.948 1.002 *** End of Report *** ====================== Area 8 1.25 -1.323 1.5 1.75 Page 1 of 1 min Data File C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\056F5601. D Sample Name: M8_Tanvi_2 Acq. Operator : SYSTEM Acq. Instrument: 7890A GC Injection Date Seq. Line : 56 Location : 56 Inj 1 Inj Volume: 0.1 pl : C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\2JP2022.S Sequence File Method. Last changed : C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\ZJP2022.M (Sequence Method) : 9/28/2022 5:44:43 PM by SYSTEM FID1 A, Front Signal (056F5601.D) 25000 PA 20000 15000 10000 5000 1 2 3 0 4 5 : 9/28/2022 9:00:46 PM 0,25 Totals : 0.5 : : Signal 1: FID1 A, Front Signal Peak RetTime Type Width # [min] [min] ==================== Area Percent Report ======== Sorted By Multiplier Dilution : Do not use Multiplier & Dilution Factor with ISTDS Signal 1.0000 1.0000 0.75 Area [pA*s] 0.835 Height [pA]: 7890A GC 9/28/2022 9:02:46 PM SYSTEM -0:910 5.89015e4 5.33811e4 0.835 BB 0.910 BB S 0.948 BV T 0.0112 2.52255 3.68258 0.00428 0.0119 2.09005e4 2.81609e4 35.48378 0.0121 128.53427 168.70262 0.21822 1.002 VB T 0.0134 1.28819 1.59166 0.00219 1.323 BB S 0.0224 3.78686e4 2.50462e4 64.29153 0.948 1.002 *** End of Report *** ====================== Area 8 1.25 -1.323 1.5 1.75 Page 1 of 1 min Data File C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-431058F5801.D Sample Name: M8_Nan_2 ================== Acq. Operator : SYSTEM Acq. Instrument: 7890A GC Injection Date Sequence File Method Last changed PA 30000 25000 20000 15000 10000 5000 0- : 9/28/2022 9:07:49 PM 1 2 3 FID1 A, Front Signal (058F5801.D) ======================== : C:\Chem32\1\Data\ZJP2022 : C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\ZJP2022.M (Sequence Method) : 9/28/2022 5:44:43 PM by SYSTEM 0.25 ========================== Totals : 0.5 ---| 0.831 BB 0.906 BB S 0.943 BV T 4 0.997 VB T 5 1.328 BB S 6 1.808 BB 7 1.944 BBA 0.0321 ========= Signal 1: FID1 A, Front Signal Peak RetTime Type Width # [min] Signal 1.0000 1.0000 ====== Area Percent Report Area [min] [pA*s] Sorted By : Multiplier : Dilution : Do not use Multiplier & Dilution Factor with ISTDS Seq. Line : 58 Location 58 Inj 1 Inj Volume: 0.1 l 2022-09-28 17-44-43\ZJP2022.S 0.75 0.831 7890A GC 9/28/2022 9:09:49 PM SYSTEM Height [pA] 0.906 7.51547e4 5.92106e4 0.943 0.997 0.0103 2.26714 3.34008 0.00302 0.0119 1.89073e4 2.54726e4 25.15779 0.0116 97.17658 135.64146 0.12930 0.0110 1.20740 1.81452 0.00161 0.0251 5.61313e4 3.35893e4 74.68768 0.0302 11.09159 5.83571 0.01476 2.12553 0.00585 4.39586 Area 8 1.25 1.328 ============== ============= 1.5 Page 1.75 1.808 1 of 2 1.944 min Data File C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\059F5901. D. Sample Name: M8_EE_1 Acq. Operator : SYSTEM Acq. Instrument: 7890A GC Injection Date Sequence File Method Last changed PA 60000 50000 40000 30000 20000 10000 0 ============ -1 1 2 3 4 FID1 A, Front Signal (059F5901.D) : 9/28/2022 9:11:21 PM 0.781 BB Totals : Inj Volume: 0.1 l : C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\ZJP2022.S : C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\ZJP2022.M (Sequence Method) : 9/28/2022 5:44:43 PM by SYSTEM 0.25 =========== Signal 1: FID1 A, Front Signal Peak RetTime Type Width # [min] [min] |-| 0.913 BB S 0.947 BB T 1.313 BB S Sorted By Multiplier Dilution : Do not use Multiplier & Dilution Factor with ISTDS. : : 0.5 Area Percent Report ---| Signal 1.0000 1.0000 0.781 Area [pA*s] 0.75 7890A GC 9/28/2022 9:13:21 PM SYSTEM 0.913 Height [pA] 6.94330e4 7.79725e4 Seq. Line : 59 Location : 59 Inj: 1 0.947 =========================== 8.15e-3 2.88223 5.84766 0.00415 0.0122 4.65751e4 6.04475e4 67.07928 0.0109 37.20157 56.93329 0.05358 0.0200 2.28177e4 1.74622e4 32.86299 *** End of Report *** Area 8 1.25 1.313 ========== ============================ 1.5 Page 1.75 1 of 1 mi Data File C:\Chem32\1\Data\ZJP2022 2022-09-28, 17-44-43\060F6001. D Sample Name: M8_EE_2 Acq. Operator : SYSTEM Acq. Instrument: 7890A GC Injection Date ==== Sequence File Method. Last changed 25000 PA 20000 15000 10000 5000 0 1 2 3 Sorted By Multiplier Dilution 4 5 : 9/28/2022 9:14:55 PM : 9/28/2022 5:44:43 PM by SYSTEM FID1 A, Front Signal (060F6001.D) 0.25 Totals : : C:\Chem32\1\Data\ZJP2022 : C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\ZJP2022.M (Sequence Method) 0.5 ============================================== Signal 1: FID1 A, Front Signal Peak RetTime Type Width # [min] [min] 0.782 BB 0.910 BBS 0.947 BB T 1.326 BB S 1.811 BB Signal 1.0000 1.0000 ==============: 0.782 0.75 Inj Volume: 0.1 pl 2022-09-28 17-44-43\ZJP2022.s Area Percent Report Area [pA*s] : : : Do not use Multiplier & Dilution Factor with ISTDS. Height [pA] Seq. Line : 60 Location : 60 Inj: 1 0.910 0.947 6.60335e4 5.81908e4 Area 8 8.56e-3 1.17570 2.22699 0.00178 0.0117 2.13307e4 2.92862e4 32.30279 0.0113 20.03166 29.42606 0.03034 0.0237 4.46760e4 2.88701e4 67.65664 0.0308 2.85511 0.00845 5.57886 1 1.25 1.5 1.75 1.811 min Data File C:\Chem32\1\Data\ZJP2022 2022-09-28, 17-44-43\060F6001. D Sample Name: M8_EE_2 Acq. Operator : SYSTEM Acq. Instrument: 7890A GC Injection Date ==== Sequence File Method. Last changed 25000 PA 20000 15000 10000 5000 0 1 2 3 Sorted By Multiplier Dilution 4 5 : 9/28/2022 9:14:55 PM : 9/28/2022 5:44:43 PM by SYSTEM FID1 A, Front Signal (060F6001.D) 0.25 Totals : : C:\Chem32\1\Data\ZJP2022 : C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\ZJP2022.M (Sequence Method) 0.5 ============================================== Signal 1: FID1 A, Front Signal Peak RetTime Type Width # [min] [min] 0.782 BB 0.910 BBS 0.947 BB T 1.326 BB S 1.811 BB Signal 1.0000 1.0000 ==============: 0.782 0.75 Inj Volume: 0.1 pl 2022-09-28 17-44-43\ZJP2022.s Area Percent Report Area [pA*s] : : : Do not use Multiplier & Dilution Factor with ISTDS. Height [pA] Seq. Line : 60 Location : 60 Inj: 1 0.910 0.947 6.60335e4 5.81908e4 Area 8 8.56e-3 1.17570 2.22699 0.00178 0.0117 2.13307e4 2.92862e4 32.30279 0.0113 20.03166 29.42606 0.03034 0.0237 4.46760e4 2.88701e4 67.65664 0.0308 2.85511 0.00845 5.57886 1 1.25 1.5 1.75 1.811 min Data File C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\062F6201. D Sample Name: M8_MA_1 Acq. Operator : SYSTEM Acq. Instrument: 7890A GC Injection Date. :9/28/2022 9:22:02 PM: Sequence File Method Last changed pA 30000 25000 20000 15000 10000 5000 0 FID1 A, Front Signal (062F6201.D) ======================= Sorted By Multiplier Dilution 1 2 3 4 5 6 ========================= Inj Volume 0.1 pl : C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\ZJP2022.S : C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\ZJP2022.M (Sequence Method) :9/28/2022 5:44:43 PM by SYSTEM 0.25 Totals : 0.836 BB 0.912 BB S 0.949 BV T 1.003 VB T 1.324 BB S 1.814 BB 0.5 2.00 Signal 1: FID1 A, Front Signal Peak RetTime Type Width # [min] ============ ========================= Signal 1.0000 1.0000 Area Percent Report 0.75 Area [min] [pA*s] : : Do not use Multiplier & Dilution Factor with ISTDS 0.836 7890A GC 9/28/2022 9:24:02 PM SYSTEM 62 Seq. Line : Location : 62 Inj : 1 -0.912 ========================================= Height [pA] 6.432014 5.72251e4 0.949 1.003 0.0106 3.03538 4.33642 0.00472 0.0126 2.49610e4 3.11365e4 38.80741 0.0121 128.86256 169.37579 0.20035 0.0132 3.68099 0.00490 0.0225 3.92203e4 2.59093e4 60.97669 0.0315 3.14920 3.81792 1.89839 0.00594 Area 8 1.25 1.324 ============== =========== 1.5 Page 1.75 1.814 1 of 2 mir Data File C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\063F6301. D Sample Name: M8_KN_1 Seq. Line : 63 Location: 63 Inj 1 Inj Volume: 0.1 l : C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\ZJP2022.S Sequence File Method Last changed : C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\ZJP2022.M (Sequence Method) : 9/28/2022 5:44:43 PM by SYSTEM FID1 A, Front Signal (063F6301.D) Acq. Operator : SYSTEM Acq. Instrument : 7890A GC Injection Date PA 50000 40000 30000 20000 10000 0 ESSES: : 9/28/2022 9:25:34 PM 0.25 0.797 VV 0.832 VB Totals : |----| 0.910 BB S 0.945 BV T 0.998 VB T 1.312 BB S 0.5 : : Signal 1: FID1 A, Front Signal Peak RetTime Type Width # [min] [min] ----|- 1 2 3 4 5 6 Sorted By Multiplier Dilution : Do not use Multiplier & Dilution Factor with ISTDS Signal 1.0000 1.0000 Area Percent Report ============================== Area [pA*s] 0.75 0.797 0.832 6.20662e4 7890A GC 9/28/2022 9:27:34 PM SYSTEM 0.910 Height [pA] $0.945 0.998 0.0101 1.07229 1.81434 0.00173 5.93362 0/8.90317 0.00956 0.0110 0.0117 3.72760e4 5.13142e4 60.05843 0.0116 200.28343 279.08847 0.32269 0.0118 2.18857 0.00260 0.0200 2.45813e4 1.88190e4 39.60499 1.61339 7.04251e4 Area 8 1.25 1.312 =========== ================================ 1.5 Page 1.75 1 of 2 min Data File C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\064F6401. D Sample Name: M8 KN 2 Acq. Operator : SYSTEM Acq. Instrument : 7890A GC Injection Date Sequence File Method Last changed PA 25000 20000 15000 10000 5000 0 Seq. Line : 64 Location: 64 Inj: 1 Inj Volume: 0.1 pl : C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\ZJP2022.S : C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\ZJP2022.M (Sequence Method) :9/28/2022 5:44:43 PM by SYSTEM 3 4 5 : 9/28/2022 9:29:06 PM: FID1 A, Front Signal (064F6401.D) ========================: 0.25 Totals : 0.5 -|- 0.908 BB S 1 2 0.947 BV T 1.001 VB T 1.325 BB S 1.811 BB Signal 1: FID1 A, Front Signal Peak RetTime Type Width Area [min] [pA*s] # [min] Area Percent Report 0.75 Sorted By : Multiplier : Dilution : Do not use Multiplier & Dilution Factor with ISTDS. Signal 1.0000 1.0000 ====================: -0.908 ===================================================== Height [PA] 0.947 1.001 ============================ 5.58922e4 4.55066e4 0.0105 1.15616e4 1.65566e4 20.68562 0.0117 83.55067 114.15410 0.14949 0.0121 1.29179 1.69159 0.00231 0.0227 4.42407e4 2.88315e4 79.15360 0.0304 5.02151 2.61823 0.00898 ============ Area 8 *** End of Report *** 1.25 4:325 ======================= 1.5 1.75 1.811 min Data File C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\065F6501. D Sample Name: M8_KC_1 ==================== Acq. Operator : SYSTEM Acq. Instrument: 7890A GC Injection Date : 9/28/2022 9:32:38 PM Sequence File Method Last changed 40000 PA 35000 30000 25000 20000 15000 10000 5000 0 - 1 1 ===================== 0.25 : 9/28/2022 5:44:43 PM by SYSTEM FID1 A, Front Signal (065F6501.D) Totals : Signal 1: FID1 A, Front Signal Peak RetTime Type Width # [min] 0.781 BB 2 0.834 BB 3 0.911 BB S 4 0.947 BV T 5 1.315 BB S : C:\Chem32\1\Data\ZJP2022 : C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\ZJP2022.M (Sequence Method) 0.5 ================ Signal 1.0000 1.0000 Area [min] [pA*s] Sorted By : Multiplier : Dilution : Do not use Multiplier & Dilution Factor with ISTDS =========================== 0.781 0.834 0.75 ===================================================================== Area Percent Report Inj : 1 Inj Volume: 0.1 ul 2022-09-28 17-44-43\ZJP2022.S 7890A GC 9/28/2022 9:34:38 PM SYSTEM -0.911 Seq. Line : Location : Height [pA] 5.67783e4 6.05619e4 0.947 8.97e-3 2.06110 3.65906 0.00363 0.0109 8.71784 013.16508 0.01535 0.0122 3.24656e4 4.19134e4 57.17959 0.0118 151.37520 206.44443 0.26661 0.0201 2.41506e4 1.84253e4 42.53482 ========= *** End of Report *** 65 ======================== Area 8 65 1.25 1.315 ============================== 1.5 Page 1.75 1 of 1 min Data File C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\066F6601.D Sample Name: M8_KC_2 =============== Acq. Operator : SYSTEM Acq. Instrument : 7890A GC Injection Date PA] Inj Volume: 0.1 pl : C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\ZJP2022.S Sequence File Method Last changed : C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\ZJP2022.M (Sequence Method) : 9/28/2022 5:44:43 PM by SYSTEM FID1 A, Front Signal (066F6601.D) 30000 25000 20000 15000 10000 5000 0 ============= : 9/28/2022 9:36:09 PM ============= 0.25 Totals : |----| 0.835 BB 0.910 BB S 0.948 BV T 1.328 BB S 1.812 BB ================ 0.5 : : Signal 1: FID1 A, Front Signal Peak RetTime Type Width # [min] |- 1 2 3 4 5 Sorted By Multiplier Dilution : Do not use Multiplier & Dilution Factor with ISTDS Area Percent Report Signal 1.0000 1.0000 0.75 0.835 Area [min] [pA*s] ============================================ -0.910 7890A GC 9/28/2022 9:38:09 PM SYSTEM ========================== Height [pA] 66 Seq. Line : Location : 66 Inj: 1 0.948 6.40644e4 5.0982404 0.0101 1.77529 2.68687 0.00277 0.0118 1.50044e4 2002882e4 23.42085 0.0119 85.36948 114.98862 0.13326 0.0243 4.89679e4 3.05741e4 76.43540 0.0312 4.95179 2.49068 0.00773 *** End of Report *** 1.25 Area ======================== 1.5 1.75 1.812 Page 1 of 1 min Question 4: Fractional distillation is performed when two or more miscible compounds have a boiling point difference (A bp) less than 40 C. 2-Methylpentane and cyclohexane boil at 62 C and 80.7 C, respectively. Given gas chromatography (GC) data from your instructor, calculate the percent composition of each compound in Frxn 1 and Frxn 2. (X% 2-methylpentane: X% cyclohexane) [Note: Area = h width at h] Frxn 1 Peak 1 (2-Methylpentane) Peak 2 (Cyclohexane) Frxn 2 Peak 1 (2-Methylpentane) Peak 2 (Cyclohexane) Peak Height (h) mm mm Peak Height (h) mm mm Peak Width at Half Height mm mm Peak Width at Half Height mm mm Data File C:\Chem32\1\Data\ZJP2022 Sample Name: M8 DB 1 www Acq. Operator : SYSTEM Acq. Instrument : 7890A GC Injection Date Sequence File Method Last changed PA 40000 30000 20000 10000 0 ================: 1 2 3 4 5 FID1 A, Front Signal (053F5301.D) Totals : : 9/28/2022 8:50:12 PM 0.25 0.5 2022-09-28 17-44-43\053F5301. D CHE.231L.1 m@8? Inj Volume 0.1 ul : C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\ZJP2022.S : C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\ZJP2022.M (Sequence Method) : 9/28/2022 5:44:43 PM by SYSTEM Signal 1: FID1 A, Front Signal Peak RetTime Type Width # [min] [min] ||----| 0.777 BB 0.835 BB 0.912 BB S 0.948 BV T 1.315 BB S ======================= =================== 1920 Signal 1.0000 1.0000 Area Percent Report Area [pA*s] 0.777 0.835 Sorted By Multiplier : Dilution. : Do not use Multiplier & Dilution Factor with ISTDS 0.75 7890A GC 9/28/2022 8:52:12 PM SYSTEM =================================================== 0:912 Height [PA] 5.96839e4 6.64521e4 0.948 Seq. Line : 53 Location : 53 1 Inj: 7.99e-3 35.09433 73.25616 0.05880 0.0108 10.47289 15.99453 0.01755 0.0117 3.43577e4 4.72489e4 57.56605 0.0115 158.73891 223.91490 0.26597 0.0203 2.51219e4 1.88901e4 42.09164 *** End of Report *** Area 8 9.26.2022 GC Data For Exp. III Fractional Distillation 1.25 -1.315 1.5 -2-Methylpentane Cyclohexane =================== Page 1.75 1 of 1 m Data File C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\054F5401. D. Sample Name: M8_DB_2 ========== Acq. Operator : SYSTEM Acq. Instrument: 7890A GC Injection Date. : 9/28/2022 8:53:43 PM Sequence File Method Last changed pA 25000 20000 15000 10000 5000 0 Seq. Line : 54 Location : 54 Inj: 1 Inj Volume : 2022-09-28 17-44-43\ZJP2022.S : C:\Chem32\1\Data\ZJP2022 : C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\ZJP2022.M (Sequence Method) : 9/28/2022 5:44:43 PM by SYSTEM FID1 A, Front Signal (054F5401.D) Sorted By Multiplier Dilution 1 2 3 4 5 =================================== 0.25 ====================================== Totals : 0.5 : ============== Signal 1: FID1 A, Front Signal Peak RetTime Type Width # [min] ||-- 0.782 BB 8.75e-3 0.835 BB 0.910 BBS 0.947 BV T 1.323 BBS Signal 1.0000 1.0000 Area Percent Report Area [min] [pA*s] 429 0.782 0.835 : Do not use Multiplier & Dilution Factor with ISTDS 0.75 7890A GC 9/28/2022 8:55:43 PM SYSTEM 0.910 Height [PA] 5.89955e4 5.34101e4 $0.947 ================ 13 s 2 m === 1.77066 3.25276 0.00300 0.0111 2.45555 3.64279 0.00416 0.0118 1.96600e4 2.67821e4 33.32452 0.0120 111.55967 147.61584 0.18910 0.0229 3.92198e4 2.64735e4 66.47922 End of Report *** 0.1 ====================== Area 8 1.25 323 ======================== 1.5 Page 1.75 1 of 1 min Data File C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\055F5501. D Sample Name: M8_Tanvi_1 Acq. Operator : SYSTEM Acq. Instrument : 7890A GC Injection Date: Sequence File Method Last changed PA 35000 30000 25000 20000 15000 10000 5000 0 =========== 1 2 3 4 5 ================== : 9/28/2022 8:57:15 PM FID1 A, Front Signal (055F5501.D) 0.780 BB 0.833 BB Totals : 0.25 : C:\Chem32\1\Data\ZJP2022 : C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\ZJP2022.M (Sequence Method) : 9/28/2022 5:44:43 PM by SYSTEM 0.909 BB S 0.945 BB T 1.305 BB S Signal 1: FID1 A, Front Signal Peak RetTime Type # [min] ----| 0.5 Width [min] | Sorted By : Multiplier : Dilution : Do not use Multiplier & Dilution Factor with ISTDS. Area Percent Report Signal 1.0000 1.0000 Inj Volume 0.1 l 2022-09-28 17-44-43\ZJP2022.S 0.780 0.833 0.75 Area [pA*s] ========================= 0.909 Height [pA] 7890A GC 9/28/2022 8:59:15 PM SYSTEM Seq. Line : 55 Location : 55 Inj: 1 3.99095e4 4.55234e4 0.945 9.46e-3 1.11849 1.84932 0.00280 7.84525 11.69148 0.01966 0.0102 0.0123 2.72068e4 3.50337e4 68.17138 0.0116 121.41135 168.12975 0.30422 0.0190 1.25723e4 1.03080e4 31.50194 ***End of Report *** Area 8 1.25 1.305 ================ ================ ============ ============= 1.5 Page 1.75 1 of 1 min Data File C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\056F5601. D Sample Name: M8_Tanvi_2 Acq. Operator : SYSTEM Acq. Instrument: 7890A GC Injection Date Seq. Line : 56 Location : 56 Inj 1 Inj Volume: 0.1 pl : C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\2JP2022.S Sequence File Method. Last changed : C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\ZJP2022.M (Sequence Method) : 9/28/2022 5:44:43 PM by SYSTEM FID1 A, Front Signal (056F5601.D) 25000 PA 20000 15000 10000 5000 1 2 3 0 4 5 : 9/28/2022 9:00:46 PM 0,25 Totals : 0.5 : : Signal 1: FID1 A, Front Signal Peak RetTime Type Width # [min] [min] ==================== Area Percent Report ======== Sorted By Multiplier Dilution : Do not use Multiplier & Dilution Factor with ISTDS Signal 1.0000 1.0000 0.75 Area [pA*s] 0.835 Height [pA]: 7890A GC 9/28/2022 9:02:46 PM SYSTEM -0:910 5.89015e4 5.33811e4 0.835 BB 0.910 BB S 0.948 BV T 0.0112 2.52255 3.68258 0.00428 0.0119 2.09005e4 2.81609e4 35.48378 0.0121 128.53427 168.70262 0.21822 1.002 VB T 0.0134 1.28819 1.59166 0.00219 1.323 BB S 0.0224 3.78686e4 2.50462e4 64.29153 0.948 1.002 *** End of Report *** ====================== Area 8 1.25 -1.323 1.5 1.75 Page 1 of 1 min Data File C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\056F5601. D Sample Name: M8_Tanvi_2 Acq. Operator : SYSTEM Acq. Instrument: 7890A GC Injection Date Seq. Line : 56 Location : 56 Inj 1 Inj Volume: 0.1 pl : C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\2JP2022.S Sequence File Method. Last changed : C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\ZJP2022.M (Sequence Method) : 9/28/2022 5:44:43 PM by SYSTEM FID1 A, Front Signal (056F5601.D) 25000 PA 20000 15000 10000 5000 1 2 3 0 4 5 : 9/28/2022 9:00:46 PM 0,25 Totals : 0.5 : : Signal 1: FID1 A, Front Signal Peak RetTime Type Width # [min] [min] ==================== Area Percent Report ======== Sorted By Multiplier Dilution : Do not use Multiplier & Dilution Factor with ISTDS Signal 1.0000 1.0000 0.75 Area [pA*s] 0.835 Height [pA]: 7890A GC 9/28/2022 9:02:46 PM SYSTEM -0:910 5.89015e4 5.33811e4 0.835 BB 0.910 BB S 0.948 BV T 0.0112 2.52255 3.68258 0.00428 0.0119 2.09005e4 2.81609e4 35.48378 0.0121 128.53427 168.70262 0.21822 1.002 VB T 0.0134 1.28819 1.59166 0.00219 1.323 BB S 0.0224 3.78686e4 2.50462e4 64.29153 0.948 1.002 *** End of Report *** ====================== Area 8 1.25 -1.323 1.5 1.75 Page 1 of 1 min Data File C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-431058F5801.D Sample Name: M8_Nan_2 ================== Acq. Operator : SYSTEM Acq. Instrument: 7890A GC Injection Date Sequence File Method Last changed PA 30000 25000 20000 15000 10000 5000 0- : 9/28/2022 9:07:49 PM 1 2 3 FID1 A, Front Signal (058F5801.D) ======================== : C:\Chem32\1\Data\ZJP2022 : C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\ZJP2022.M (Sequence Method) : 9/28/2022 5:44:43 PM by SYSTEM 0.25 ========================== Totals : 0.5 ---| 0.831 BB 0.906 BB S 0.943 BV T 4 0.997 VB T 5 1.328 BB S 6 1.808 BB 7 1.944 BBA 0.0321 ========= Signal 1: FID1 A, Front Signal Peak RetTime Type Width # [min] Signal 1.0000 1.0000 ====== Area Percent Report Area [min] [pA*s] Sorted By : Multiplier : Dilution : Do not use Multiplier & Dilution Factor with ISTDS Seq. Line : 58 Location 58 Inj 1 Inj Volume: 0.1 l 2022-09-28 17-44-43\ZJP2022.S 0.75 0.831 7890A GC 9/28/2022 9:09:49 PM SYSTEM Height [pA] 0.906 7.51547e4 5.92106e4 0.943 0.997 0.0103 2.26714 3.34008 0.00302 0.0119 1.89073e4 2.54726e4 25.15779 0.0116 97.17658 135.64146 0.12930 0.0110 1.20740 1.81452 0.00161 0.0251 5.61313e4 3.35893e4 74.68768 0.0302 11.09159 5.83571 0.01476 2.12553 0.00585 4.39586 Area 8 1.25 1.328 ============== ============= 1.5 Page 1.75 1.808 1 of 2 1.944 min Data File C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\059F5901. D. Sample Name: M8_EE_1 Acq. Operator : SYSTEM Acq. Instrument: 7890A GC Injection Date Sequence File Method Last changed PA 60000 50000 40000 30000 20000 10000 0 ============ -1 1 2 3 4 FID1 A, Front Signal (059F5901.D) : 9/28/2022 9:11:21 PM 0.781 BB Totals : Inj Volume: 0.1 l : C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\ZJP2022.S : C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\ZJP2022.M (Sequence Method) : 9/28/2022 5:44:43 PM by SYSTEM 0.25 =========== Signal 1: FID1 A, Front Signal Peak RetTime Type Width # [min] [min] |-| 0.913 BB S 0.947 BB T 1.313 BB S Sorted By Multiplier Dilution : Do not use Multiplier & Dilution Factor with ISTDS. : : 0.5 Area Percent Report ---| Signal 1.0000 1.0000 0.781 Area [pA*s] 0.75 7890A GC 9/28/2022 9:13:21 PM SYSTEM 0.913 Height [pA] 6.94330e4 7.79725e4 Seq. Line : 59 Location : 59 Inj: 1 0.947 =========================== 8.15e-3 2.88223 5.84766 0.00415 0.0122 4.65751e4 6.04475e4 67.07928 0.0109 37.20157 56.93329 0.05358 0.0200 2.28177e4 1.74622e4 32.86299 *** End of Report *** Area 8 1.25 1.313 ========== ============================ 1.5 Page 1.75 1 of 1 mi Data File C:\Chem32\1\Data\ZJP2022 2022-09-28, 17-44-43\060F6001. D Sample Name: M8_EE_2 Acq. Operator : SYSTEM Acq. Instrument: 7890A GC Injection Date ==== Sequence File Method. Last changed 25000 PA 20000 15000 10000 5000 0 1 2 3 Sorted By Multiplier Dilution 4 5 : 9/28/2022 9:14:55 PM : 9/28/2022 5:44:43 PM by SYSTEM FID1 A, Front Signal (060F6001.D) 0.25 Totals : : C:\Chem32\1\Data\ZJP2022 : C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\ZJP2022.M (Sequence Method) 0.5 ============================================== Signal 1: FID1 A, Front Signal Peak RetTime Type Width # [min] [min] 0.782 BB 0.910 BBS 0.947 BB T 1.326 BB S 1.811 BB Signal 1.0000 1.0000 ==============: 0.782 0.75 Inj Volume: 0.1 pl 2022-09-28 17-44-43\ZJP2022.s Area Percent Report Area [pA*s] : : : Do not use Multiplier & Dilution Factor with ISTDS. Height [pA] Seq. Line : 60 Location : 60 Inj: 1 0.910 0.947 6.60335e4 5.81908e4 Area 8 8.56e-3 1.17570 2.22699 0.00178 0.0117 2.13307e4 2.92862e4 32.30279 0.0113 20.03166 29.42606 0.03034 0.0237 4.46760e4 2.88701e4 67.65664 0.0308 2.85511 0.00845 5.57886 1 1.25 1.5 1.75 1.811 min Data File C:\Chem32\1\Data\ZJP2022 2022-09-28, 17-44-43\060F6001. D Sample Name: M8_EE_2 Acq. Operator : SYSTEM Acq. Instrument: 7890A GC Injection Date ==== Sequence File Method. Last changed 25000 PA 20000 15000 10000 5000 0 1 2 3 Sorted By Multiplier Dilution 4 5 : 9/28/2022 9:14:55 PM : 9/28/2022 5:44:43 PM by SYSTEM FID1 A, Front Signal (060F6001.D) 0.25 Totals : : C:\Chem32\1\Data\ZJP2022 : C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\ZJP2022.M (Sequence Method) 0.5 ============================================== Signal 1: FID1 A, Front Signal Peak RetTime Type Width # [min] [min] 0.782 BB 0.910 BBS 0.947 BB T 1.326 BB S 1.811 BB Signal 1.0000 1.0000 ==============: 0.782 0.75 Inj Volume: 0.1 pl 2022-09-28 17-44-43\ZJP2022.s Area Percent Report Area [pA*s] : : : Do not use Multiplier & Dilution Factor with ISTDS. Height [pA] Seq. Line : 60 Location : 60 Inj: 1 0.910 0.947 6.60335e4 5.81908e4 Area 8 8.56e-3 1.17570 2.22699 0.00178 0.0117 2.13307e4 2.92862e4 32.30279 0.0113 20.03166 29.42606 0.03034 0.0237 4.46760e4 2.88701e4 67.65664 0.0308 2.85511 0.00845 5.57886 1 1.25 1.5 1.75 1.811 min Data File C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\062F6201. D Sample Name: M8_MA_1 Acq. Operator : SYSTEM Acq. Instrument: 7890A GC Injection Date. :9/28/2022 9:22:02 PM: Sequence File Method Last changed pA 30000 25000 20000 15000 10000 5000 0 FID1 A, Front Signal (062F6201.D) ======================= Sorted By Multiplier Dilution 1 2 3 4 5 6 ========================= Inj Volume 0.1 pl : C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\ZJP2022.S : C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\ZJP2022.M (Sequence Method) :9/28/2022 5:44:43 PM by SYSTEM 0.25 Totals : 0.836 BB 0.912 BB S 0.949 BV T 1.003 VB T 1.324 BB S 1.814 BB 0.5 2.00 Signal 1: FID1 A, Front Signal Peak RetTime Type Width # [min] ============ ========================= Signal 1.0000 1.0000 Area Percent Report 0.75 Area [min] [pA*s] : : Do not use Multiplier & Dilution Factor with ISTDS 0.836 7890A GC 9/28/2022 9:24:02 PM SYSTEM 62 Seq. Line : Location : 62 Inj : 1 -0.912 ========================================= Height [pA] 6.432014 5.72251e4 0.949 1.003 0.0106 3.03538 4.33642 0.00472 0.0126 2.49610e4 3.11365e4 38.80741 0.0121 128.86256 169.37579 0.20035 0.0132 3.68099 0.00490 0.0225 3.92203e4 2.59093e4 60.97669 0.0315 3.14920 3.81792 1.89839 0.00594 Area 8 1.25 1.324 ============== =========== 1.5 Page 1.75 1.814 1 of 2 mir Data File C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\063F6301. D Sample Name: M8_KN_1 Seq. Line : 63 Location: 63 Inj 1 Inj Volume: 0.1 l : C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\ZJP2022.S Sequence File Method Last changed : C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\ZJP2022.M (Sequence Method) : 9/28/2022 5:44:43 PM by SYSTEM FID1 A, Front Signal (063F6301.D) Acq. Operator : SYSTEM Acq. Instrument : 7890A GC Injection Date PA 50000 40000 30000 20000 10000 0 ESSES: : 9/28/2022 9:25:34 PM 0.25 0.797 VV 0.832 VB Totals : |----| 0.910 BB S 0.945 BV T 0.998 VB T 1.312 BB S 0.5 : : Signal 1: FID1 A, Front Signal Peak RetTime Type Width # [min] [min] ----|- 1 2 3 4 5 6 Sorted By Multiplier Dilution : Do not use Multiplier & Dilution Factor with ISTDS Signal 1.0000 1.0000 Area Percent Report ============================== Area [pA*s] 0.75 0.797 0.832 6.20662e4 7890A GC 9/28/2022 9:27:34 PM SYSTEM 0.910 Height [pA] $0.945 0.998 0.0101 1.07229 1.81434 0.00173 5.93362 0/8.90317 0.00956 0.0110 0.0117 3.72760e4 5.13142e4 60.05843 0.0116 200.28343 279.08847 0.32269 0.0118 2.18857 0.00260 0.0200 2.45813e4 1.88190e4 39.60499 1.61339 7.04251e4 Area 8 1.25 1.312 =========== ================================ 1.5 Page 1.75 1 of 2 min Data File C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\064F6401. D Sample Name: M8 KN 2 Acq. Operator : SYSTEM Acq. Instrument : 7890A GC Injection Date Sequence File Method Last changed PA 25000 20000 15000 10000 5000 0 Seq. Line : 64 Location: 64 Inj: 1 Inj Volume: 0.1 pl : C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\ZJP2022.S : C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\ZJP2022.M (Sequence Method) :9/28/2022 5:44:43 PM by SYSTEM 3 4 5 : 9/28/2022 9:29:06 PM: FID1 A, Front Signal (064F6401.D) ========================: 0.25 Totals : 0.5 -|- 0.908 BB S 1 2 0.947 BV T 1.001 VB T 1.325 BB S 1.811 BB Signal 1: FID1 A, Front Signal Peak RetTime Type Width Area [min] [pA*s] # [min] Area Percent Report 0.75 Sorted By : Multiplier : Dilution : Do not use Multiplier & Dilution Factor with ISTDS. Signal 1.0000 1.0000 ====================: -0.908 ===================================================== Height [PA] 0.947 1.001 ============================ 5.58922e4 4.55066e4 0.0105 1.15616e4 1.65566e4 20.68562 0.0117 83.55067 114.15410 0.14949 0.0121 1.29179 1.69159 0.00231 0.0227 4.42407e4 2.88315e4 79.15360 0.0304 5.02151 2.61823 0.00898 ============ Area 8 *** End of Report *** 1.25 4:325 ======================= 1.5 1.75 1.811 min Data File C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\065F6501. D Sample Name: M8_KC_1 ==================== Acq. Operator : SYSTEM Acq. Instrument: 7890A GC Injection Date : 9/28/2022 9:32:38 PM Sequence File Method Last changed 40000 PA 35000 30000 25000 20000 15000 10000 5000 0 - 1 1 ===================== 0.25 : 9/28/2022 5:44:43 PM by SYSTEM FID1 A, Front Signal (065F6501.D) Totals : Signal 1: FID1 A, Front Signal Peak RetTime Type Width # [min] 0.781 BB 2 0.834 BB 3 0.911 BB S 4 0.947 BV T 5 1.315 BB S : C:\Chem32\1\Data\ZJP2022 : C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\ZJP2022.M (Sequence Method) 0.5 ================ Signal 1.0000 1.0000 Area [min] [pA*s] Sorted By : Multiplier : Dilution : Do not use Multiplier & Dilution Factor with ISTDS =========================== 0.781 0.834 0.75 ===================================================================== Area Percent Report Inj : 1 Inj Volume: 0.1 ul 2022-09-28 17-44-43\ZJP2022.S 7890A GC 9/28/2022 9:34:38 PM SYSTEM -0.911 Seq. Line : Location : Height [pA] 5.67783e4 6.05619e4 0.947 8.97e-3 2.06110 3.65906 0.00363 0.0109 8.71784 013.16508 0.01535 0.0122 3.24656e4 4.19134e4 57.17959 0.0118 151.37520 206.44443 0.26661 0.0201 2.41506e4 1.84253e4 42.53482 ========= *** End of Report *** 65 ======================== Area 8 65 1.25 1.315 ============================== 1.5 Page 1.75 1 of 1 min Data File C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\066F6601.D Sample Name: M8_KC_2 =============== Acq. Operator : SYSTEM Acq. Instrument : 7890A GC Injection Date PA] Inj Volume: 0.1 pl : C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\ZJP2022.S Sequence File Method Last changed : C:\Chem32\1\Data\ZJP2022 2022-09-28 17-44-43\ZJP2022.M (Sequence Method) : 9/28/2022 5:44:43 PM by SYSTEM FID1 A, Front Signal (066F6601.D) 30000 25000 20000 15000 10000 5000 0 ============= : 9/28/2022 9:36:09 PM ============= 0.25 Totals : |----| 0.835 BB 0.910 BB S 0.948 BV T 1.328 BB S 1.812 BB ================ 0.5 : : Signal 1: FID1 A, Front Signal Peak RetTime Type Width # [min] |- 1 2 3 4 5 Sorted By Multiplier Dilution : Do not use Multiplier & Dilution Factor with ISTDS Area Percent Report Signal 1.0000 1.0000 0.75 0.835 Area [min] [pA*s] ============================================ -0.910 7890A GC 9/28/2022 9:38:09 PM SYSTEM ========================== Height [pA] 66 Seq. Line : Location : 66 Inj: 1 0.948 6.40644e4 5.0982404 0.0101 1.77529 2.68687 0.00277 0.0118 1.50044e4 2002882e4 23.42085 0.0119 85.36948 114.98862 0.13326 0.0243 4.89679e4 3.05741e4 76.43540 0.0312 4.95179 2.49068 0.00773 *** End of Report *** 1.25 Area ======================== 1.5 1.75 1.812 Page 1 of 1 min