(a) Potassium iodate solution was prepared by dissolving 1.022 g of KIO3 (FM 214.00) in a 500-mL...
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(b) The triiodide from part (a) reacted with 37.66 mL of Na2S2O3 solution. What is the concentration of the Na2S2O3 solution?
(c) A 1.223-g sample of solid containing ascorbic acid and inert ingredients was dissolved in dilute H2SO4 and treated with 2 g of KI and 50.00 mL of KIO3 solution from part (a). Excess triiodide required 14.22 mL of Na2S2O3 solution from part (b). Find the weight percent of ascorbic acid (FM 176.13) in the unknown.
(d) Does it matter whether starch indicator is added at the beginning or near the end point in the titration in part (c)?
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