Experiment 5: A Separation and Purification Scheme Your mixture will be: Mixture 1 10.69 4,4 Dibremebenzeme Mixture 0.5g 1,4 Dibromobenzene Mixture 3 0.5g 1,4 Dibromobenzene 2.0g Benzoin 2.0g Benzil 2.Og Benzoin 2.5 Benzoic Acid 2.59 Benzoic Acid 2.5g Ethyl-4- Aminobenzoate 2.59 Benzil Mixture 4 0.59 4,4 Dibrorobenzone 2.Og Ethyl 4 -Aminobenzoata 2.0g-o-Toluio-Acid Tviixtures -0.5g 1,4 Dibromobenzene 2.69 Fluorone Of the three chemicals in your mixture, you need to isolate the two major components. Before performing Experiment 5, you must have two flow charts that diagram the separation of the components in your mixture. One flow chart will show this separation utilizing diethyl ether as the solvent and the other flow chart will show this separation utilizing methylene chloride as the solvent. You will NOT be allowed to perform the experiment until you have a flow chart. The degree of detail for your flow chart should be that anyone could perform the separation only using your flow chart. Page 737 of your text as well as the answer key to the extraction lab gives examples of the type of detail you should include. Each flow chart will show the following: 1. Structures of each compound at every separation stage. 2. Identity of the solvents in the upper and lower layers when two immiscible solvents are used. Your flow chart must also include steps such as drying organic solvents or separating solids from a solid liquid mixture. I encourage students to work in groups to figure out their flow charts Experiment 5: A Separation and Purification Scheme Your mixture will be: Mixture 1 10.69 4,4 Dibremebenzeme Mixture 0.5g 1,4 Dibromobenzene Mixture 3 0.5g 1,4 Dibromobenzene 2.0g Benzoin 2.0g Benzil 2.Og Benzoin 2.5 Benzoic Acid 2.59 Benzoic Acid 2.5g Ethyl-4- Aminobenzoate 2.59 Benzil Mixture 4 0.59 4,4 Dibrorobenzone 2.Og Ethyl 4 -Aminobenzoata 2.0g-o-Toluio-Acid Tviixtures -0.5g 1,4 Dibromobenzene 2.69 Fluorone Of the three chemicals in your mixture, you need to isolate the two major components. Before performing Experiment 5, you must have two flow charts that diagram the separation of the components in your mixture. One flow chart will show this separation utilizing diethyl ether as the solvent and the other flow chart will show this separation utilizing methylene chloride as the solvent. You will NOT be allowed to perform the experiment until you have a flow chart. The degree of detail for your flow chart should be that anyone could perform the separation only using your flow chart. Page 737 of your text as well as the answer key to the extraction lab gives examples of the type of detail you should include. Each flow chart will show the following: 1. Structures of each compound at every separation stage. 2. Identity of the solvents in the upper and lower layers when two immiscible solvents are used. Your flow chart must also include steps such as drying organic solvents or separating solids from a solid liquid mixture. I encourage students to work in groups to figure out their flow charts