Question: One-grams of a sediment sample was digested with 5 ml conc. HCI followed by 3 mi HNO, and then by 5 ml conc. HF and


One-grams of a sediment sample was digested with 5 ml conc. HCI followed by 3 mi HNO, and then by 5 ml conc. HF and heated to dryness, then added 10 ml d- jonized water. The sample solution filtrated into 100 ml V-flask and diluted to the mark with 1% HNO3. For quantitative analysis standards, solutions were papered and measured by flame photometer for their emission, as shown in the table below. 10. LI- Standard 0.0 1.0 2.0 4.0 8.0 10.0 (ppm) Average Emission 0.01 2.5 5.0 10.0 20.0 25.0 0) Standard 1.5x10 0.12 0.15 0.2 0.3 0.4 deviation Calculate: (Show your calculations) The concentration of Lithium (Li) in the sediment sample by ppm if the sample solution gave an average emission equal to 12.50). Calibration sensitivity Analytical sensitivity at concentration 2.0 ppm One-grams of a sediment sample was digested with 5 ml conc. HCI followed by 3 ml HNO, and then by 5 ml conc. HF and heated to dryness, then added 10 ml d- ionized water. The sample solution filtrated into 100 ml V-flask and diluted to the mark with 1% HNO3. For quantitative analysis standards, solutions were papered and measured by flame photometer for their emission, as shown in the table below. LI Standard 0.0 10 2.0 4.0 8.0 10.0 (ppm) Average Emission 0.01 2.5 5.0 10.0 20.0 25.0 U) Standard 1.5x10 0.12 0.15 0.2 0.3 0.4 deviation Calculate: (Show your calculations) The concentration of Lithium (Lit) in the sediment sample by ppm if the sample solution gave an average emission equal to 12.5.0). Calibration sensitivity Analytical sensitivity at concentration 2.0 ppm
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